1、

Methods 3-Fluoro-4-methoxybenzaldehyde was prepared through the reaction of 2-fluoroanisole with hexamethylenetetramine in the presence of trifluoroacetic acid, and then extracted with anhydrous ether from the mixture after basification with potassium carbonate.

方法以三氟乙酸为溶剂,邻氟苯甲醚与六次甲基四胺发生回流反应,通过无水碳酸钾调节酸碱度、无水乙醚萃取等操作制备3氟4甲氧基苯甲醛。

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2、

Trifluoroacetic acid ( TFA) was used as the retaining acid and ammonia liquor as the eluent base. The solvent system was n-hexane-acetic ester-methanol-water ( ratio by volume was 9 ∶ 1 ∶ 5 ∶ 5).

采用三氟乙酸做为保留酸,氨水作为洗脱碱,溶剂系统为正己烷/乙酸乙酯/甲醇/水(体积比为9∶1∶5∶5)。

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3、

Friedel-Crafts Acylation Reactions Catalyzed by Trifluoroacetic Anhydride-Synthesis of 4-Ethyl-2,5-dimethoxyphenyl Alkyl Ketones

三氟乙酸酐催化的Friedel-Crafts酰化反应&4-乙基-2,5-二甲氧基苯基烷基酮的合成

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4、

this study was focused on the determination of trace trifluoroacetic acid ( tfa) with derivation-gas chromatography.

本文研究了水中微量三氟乙酸(TFA)的衍生化-气相色谱检测方法。

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5、

For the oxidation reaction, under the conditions of 24h and room temperature, the volume proportion of trifluoroacetic acid and H_2O_2,1 ∶ 10.

氧化反应:室温条件下氧化24h,三氟乙酸与双氧水的体积比为1∶10。

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